NF ISO 22634-2

NF ISO 22634-2

May 2020
Standard Current

Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 2 : method using cyclohexane as extraction solvent

This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with cyclohexane as extraction solvent. This method is specified using ISO 3308 smoking parameters. This document provides an alternative method to that specified in ISO 22634-1, with a different clean-up, and a shorter total analytical run allowing a potential increase of sample throughput in comparison with ISO 22634-1.

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Main informations

Collections

National standards and national normative documents

Publication date

May 2020

Number of pages

16 p.

Reference

NF ISO 22634-2

ICS Codes

65.160   Tobacco, tobacco products and related equipment

Classification index

V37-050-2

Print number

1

International kinship

ISO 22634-2:2019
Sumary
Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 2 : method using cyclohexane as extraction solvent

This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography/mass spectrometry (GC/MS) with cyclohexane as extraction solvent.

This method is specified using ISO 3308 smoking parameters. This document provides an alternative method to that specified in ISO 22634-1, with a different clean-up, and a shorter total analytical run allowing a potential increase of sample throughput in comparison with ISO 22634-1.

Replaced standards (1)
NF ISO 22634-2
January 2018
Standard Cancelled
Cigarettes - Determination of benzo[a]pyrene in cigarette mainstream smoke using GC/MS - Part 2 : Method using cyclohexane as extraction solvent

Le présent document spécifie une méthode de dosage du benzo[a]pyrène (B[a]P) dans la matière particulaire totale du courant principal de la fumée de cigarette par chromatographie en phase gazeuse couplée à la spectrométrie de masse (CG/SM) en utilisant du cyclohexane comme solvant d'extraction. Cette méthode a été validée en utilisant les paramètres de fumage de la NF ISO 3308, et elle est techniquement compatible avec d'autres régimes de fumage.

Table of contents
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  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Principe
  • 5 Appareillage
  • 6 Réactifs
  • 7 Étalons
  • 8 Préparation de l'échantillon
  • 9 Dosage
  • 10 Répétabilité et reproductibilité
  • 11 Rapport d'essai
  • Annexe A Exemple de chromatogramme d'un extrait de fumée de cigarette
  • Bibliographie
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